Alumina Ball Milling Process

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Sep 01, 2016nbsp018332Further, to prevent oxidation during the ball-milling process, the grinding bowls were filled with argon gas, and a lock device was used to gas-tight seal the bowls in the glove box. The milling speed was set at 350 rpm, and the samples were taken out every 4 h for analysis until 20 h of milling had been completed.

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